4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether

Base Information

• Chemical Name: 4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether
• CAS No.: 137677-91-9
• Molecular Formula: C₁₅H₈F₁₈N₂O
• Molecular Weight: 574.213

Synonyms:4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether

Chemical Property of 4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether

Chemical Property:

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Technology Process of 4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether

There total 3 articles about 4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,3-Dinitro-2-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-octyloxy)-5-trifluoromethyl-benzene (137677-90-8) → 4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether (137677-91-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1016/S0022-1139(00)80957-4

Reference yield:

4-chloro-3,5-dinitrobenzotrifluoride (393-75-9) → 4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether (137677-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 0 deg C, 1 h, 2.) 0 deg C to r.t., 3 h

2: 93 percent / H₂ / 10percent Pd/C / ethanol

With hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;

DOI:10.1016/S0022-1139(00)80957-4

Reference yield:

2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol (307-30-2) → 4-trifluoromethyl-2,6-diaminophenyl 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyl ether (137677-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 0 deg C, 1 h, 2.) 0 deg C to r.t., 3 h

2: 93 percent / H₂ / 10percent Pd/C / ethanol

With hydrogen; sodium hydride; palladium on activated charcoal; In ethanol;

DOI:10.1016/S0022-1139(00)80957-4

upstream raw materials:

1,3-Dinitro-2-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-octyloxy)-5-trifluoromethyl-benzene

4-chloro-3,5-dinitrobenzotrifluoride

2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

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