1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol

Base Information

Chemical Name:1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol
CAS No.:1375006-69-1
Molecular Formula:C₁₅H₁₆N₁₀O₂
Molecular Weight:368.358
Hs Code.:

Synonyms:1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol

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Chemical Property of 1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol

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Technology Process of 1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol

There total 3 articles about 1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1375006-69-1
1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol

Guidance literature:: With copper diacetate; In water; at 20 ℃; for 5h;

Reference yield:

: 1375006-86-2
(1-(4-bromobutyl)-1H-1,2,3-triazol-4-yl)methanol

: 1375006-69-1
1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / dichloromethane / 19 h / 0 - 20 °C

2: sodium azide / N,N-dimethyl-formamide / 50 °C

3: copper diacetate / methanol; dichloromethane; water / 5 h / 20 °C

With sodium azide; copper diacetate; phosphorus tribromide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol300899n

Reference yield:

: 1375006-87-3
1-(4-bromobutyl)-4-(bromomethyl)-1H-1,2,3-triazole

: 1375006-69-1
1-(4-azidobutyl)4-((4-(4-nitrophenyl)-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,3-triazol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 50 °C

2: copper diacetate / methanol; dichloromethane; water / 5 h / 20 °C

With sodium azide; copper diacetate; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol300899n