5-(2-METHYL-1,3-THIAZOL-4-YL)-2-THIOPHENECARBOXYLIC ACID

Base Information

• Chemical Name: 5-(2-METHYL-1,3-THIAZOL-4-YL)-2-THIOPHENECARBOXYLIC ACID
• CAS No.: 400715-45-9
• Molecular Formula: C9H7 N O2 S2
• Molecular Weight: 225.292
• Hs Code.: 2934999090
• Mol file: 400715-45-9.mol

Synonyms:5-(2-Methylthiazol-4-yl)thiophene-2-carboxylicacid

Chemical Property of 5-(2-METHYL-1,3-THIAZOL-4-YL)-2-THIOPHENECARBOXYLIC ACID

Chemical Property:

• Vapor Pressure: 2.57E-08mmHg at 25°C
• Melting Point: 200 °C
• Refractive Index: 1.659
• Boiling Point: 434.4°Cat760mmHg
• Flash Point: 216.5°C
• PSA: 106.67000
• Density: 1.446g/cm³
• LogP: 2.87820

Purity/Quality:

98%min ^*data from raw suppliers

5-(2-methyl-1,3-thiazol-4-yl)thiophene-2-carboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.
• Hazard Codes: Xn
• Statements: 22
• Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S37/39:Wear suitable g

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(2-METHYL-1,3-THIAZOL-4-YL)-2-THIOPHENECARBOXYLIC ACID

There total 1 articles about 5-(2-METHYL-1,3-THIAZOL-4-YL)-2-THIOPHENECARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

aqueous LiOH + 5-(2-methylthiazol-4-yl)thiophen-2-carboxylic acid methyl ester (400715-92-6) → 5-(2-methyl-1,3-thiazol-4-yl)thiophen-2-carboxylic acid (400715-45-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane;

Reference yield: 61.0%

4-amino-2-methoxy-N-(3-morpholin-4-yl-propyl)-benzamide (617244-91-4) + 5-(2-methyl-1,3-thiazol-4-yl)thiophen-2-carboxylic acid (400715-45-9) → 2-methoxy-4-{3-[5-(2-methyl-thiazol-4-yl)-thiophen-2-yl]-ureido}-N-(3-morpholin-4-yl-propyl)-benzamide (617245-63-3)

Guidance literature:

5-(2-methyl-1,3-thiazol-4-yl)thiophen-2-carboxylic acid; With diphenyl phosphoryl azide; triethylamine; In toluene; for 3h; Heating / reflux;

4-amino-2-methoxy-N-(3-morpholin-4-yl-propyl)-benzamide; In dichloromethane; toluene;

upstream raw materials:

5-(2-methylthiazol-4-yl)thiophen-2-carboxylic acid methyl ester

Downstream raw materials:

2-methoxy-4-{3-[5-(2-methyl-thiazol-4-yl)-thiophen-2-yl]-ureido}-N-(3-morpholin-4-yl-propyl)-benzamide

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