(2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

Base Information

Chemical Name:(2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran
CAS No.:1065271-51-3
Molecular Formula:C₃₉H₄₈O₃Si₂
Molecular Weight:620.979
Hs Code.:

Synonyms:(2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

Suppliers and Price of (2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

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Technology Process of (2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

There total 1 articles about (2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: (2S,3R)-2-(tert-butyldiphenylsilanyloxymethyl)-3-hydroxy-4-vinyltetrahydrofuran

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1065271-51-3
(2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo801338t

Reference yield: 86.0%

: 1065271-51-3
(2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

: 1065271-52-4
(2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-formyltetrahydrofuran

Guidance literature:: (2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran; With osmium(VIII) oxide; N-methyl-2-indolinone; In water; acetone; at 20 ℃; for 2h;

With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 0.25h; Further stages.;
DOI:10.1021/jo801338t

Reference yield: 18.0%

: 111957-98-3,625-31-0
Pent-4-en-2-ol

: 1065271-51-3
(2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-vinyltetrahydrofuran

: 24218-41-5
(4E)-oct-4-ene-2,7-diol

: 1065271-60-4
(1'E,2S,3R,4S)-3-(tert-butyldiphenylsilanyloxy)-2-(tert-butyldiphenylsilanyloxymethyl)-4-(4'-hydroxy-1'-pentenyl)tetrahydrofuran

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; for 48h; Heating;
DOI:10.1021/jo801338t