(4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester

Base Information

Chemical Name:(4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester
CAS No.:630407-46-4
Molecular Formula:C₂₃H₂₉BrN₂O₄S
Molecular Weight:509.464
Hs Code.:

Synonyms:(4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester

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Technology Process of (4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester

There total 1 articles about (4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 630407-45-3
(4-Bromo-phenylsulfanyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester

: 630407-46-4
(4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester

Guidance literature:: With magnesium bis(monoperoxyphthalate)hexahydrate; In methanol; dichloromethane; at 0 - 20 ℃; for 3.25h;

Reference yield: 81.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 630407-46-4
(4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester

: 630407-42-0
[8-(4-Bromo-benzenesulfonyl)-3-methyl-2, 3,4, 5-tetrahydro-1-H-3-benzazepin-7-yl]-dimethyl-amine

Guidance literature:: (4-Bromo-benzenesulfonyl)-dimethylamino-1,2,4,5-tetrahydro-3-benzazepine-3-carboxylic acid dimethyl-ethyl ester; With hydrogenchloride; In 1,4-dioxane; ethanol; at 40 ℃; for 2h;

formaldehyd; In dichlorethane-1,2; water; at 20 ℃; for 0.333333h;

With sodium tris(acetoxy)borohydride; at 20 ℃; for 0.75h;