meso-phenyl>triphenylporphyrin

Base Information

• Chemical Name: meso-phenyl>triphenylporphyrin
• CAS No.: 80441-47-0
• Molecular Formula: C₆₈H₅₃N₅OS
• Molecular Weight: 988.268

Synonyms:meso-phenyl>triphenylporphyrin

Chemical Property of meso-phenyl>triphenylporphyrin

Chemical Property:

Purity/Quality:

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Technology Process of meso-phenyl>triphenylporphyrin

There total 4 articles about meso-phenyl>triphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

triphenylmethanethiol (3695-77-0) + meso-triphenylporphyrin (80441-46-9) → meso-phenyl>triphenylporphyrin (80441-47-0)

Guidance literature:

With potassium carbonate; In acetonitrile; for 12h; Ambient temperature;

DOI:10.1021/ja00369a041

Reference yield:

5-(2-aminophenyl)-10,15,20-triphenylporphyrinate (69082-94-6) → meso-phenyl>triphenylporphyrin (80441-47-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / pyridine / CH₂Cl₂ / 10 h / Ambient temperature

2: 64 percent / K₂CO₃ / acetonitrile / 12 h / Ambient temperature

With pyridine; potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1021/ja00369a041

Reference yield:

5-bromovaleroyl chloride (4509-90-4) → meso-phenyl>triphenylporphyrin (80441-47-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / pyridine / CH₂Cl₂ / 10 h / Ambient temperature

2: 64 percent / K₂CO₃ / acetonitrile / 12 h / Ambient temperature

With pyridine; potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1021/ja00369a041

upstream raw materials:

triphenylmethanethiol

meso-triphenylporphyrin

5-(2-aminophenyl)-10,15,20-triphenylporphyrinate

5-bromovaleroyl chloride

Downstream raw materials:

meso-triphenylporphyrin

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