2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine

Base Information

• Chemical Name: 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine
• CAS No.: 72011-33-7
• Molecular Formula: C₂₄H₂₁ClN₄O₄
• Molecular Weight: 464.908

Synonyms:2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine

Chemical Property of 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine

There total 3 articles about 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

tert-butylisonitrile (119072-55-8,7188-38-7) + 3t-(4-chloro-phenyl)-2-cyano-1-phthalimido-aziridine-2r-carboxylic acid methyl ester (49678-79-7) → phthalimide (136918-14-4,85-41-6) + 1-(methoxycarbonyl)-2-aza-1-cyano-3-(p-chlorophenyl)-4-phthalimido-4-(tert-butylamino)buta-1,3-diene (72011-42-8) + 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine (72011-33-7,84118-18-3,84118-19-4) + 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine (72011-33-7,84118-18-3,84118-19-4)

Guidance literature:

In dichloromethane; at 40 ℃; for 5h; Further byproducts given. Yields of byproduct given;

DOI:10.1021/jo00152a014

Reference yield: 15.0%

tert-butylisonitrile (119072-55-8,7188-38-7) + 3t-(4-chloro-phenyl)-2-cyano-1-phthalimido-aziridine-2r-carboxylic acid methyl ester (49678-79-7) → phthalimide (136918-14-4,85-41-6) + 1-(methoxycarbonyl)-2-aza-1-cyano-3-(p-chlorophenyl)-4-phthalimido-4-(tert-butylamino)buta-1,3-diene (72011-42-8) + 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine (72011-33-7,84118-18-3,84118-19-4) + 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine (72011-33-7,84118-18-3,84118-19-4)

Guidance literature:

In dichloromethane; at 40 ℃; for 5h; Further byproducts given. Yields of byproduct given;

DOI:10.1021/jo00152a014

Reference yield:

→ 2-cyano-2-(methoxycarbonyl)-4-(p-chlorophenyl)-1-phthalimido-3-(tert-butylimino)azetidine (72011-33-7)

Guidance literature:

t-Butylisonitril, /BRN= 501690/ (1b);

DOI:10.1016/S0040-4039(01)86156-6

upstream raw materials:

tert-butylisonitrile

3t-(4-chloro-phenyl)-2-cyano-1-phthalimido-aziridine-2r-carboxylic acid methyl ester

Downstream raw materials:

phthalimide

1-(methoxycarbonyl)-2-aza-1-cyano-3-(p-chlorophenyl)-4-phthalimido-4-(tert-butylamino)buta-1,3-diene

[(E)-(Z)-2-tert-Butylamino-1-(4-chloro-phenyl)-2-methoxy-vinylimino]-cyano-acetic acid methyl ester

N-aminophthalamide

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