Technology Process of benzyl 4-methylenecyclohexylmethylcarbamate
There total 5 articles about benzyl 4-methylenecyclohexylmethylcarbamate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / -10 - 20 °C
2: triethylamine / dichloromethane / -10 - 20 °C
With
lithium aluminium tetrahydride; triethylamine;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonia / 80 °C / Cooling
2: lithium aluminium tetrahydride / tetrahydrofuran / -10 - 20 °C
3: triethylamine / dichloromethane / -10 - 20 °C
With
lithium aluminium tetrahydride; ammonia; triethylamine;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / -20 °C
1.2: 0 - 20 °C / Inert atmosphere
2.1: water; sodium hydroxide / methanol / 0.5 h / 50 °C
3.1: dicyclohexyl-carbodiimide / dichloromethane / -10 - 20 °C
4.1: ammonia / 80 °C / Cooling
5.1: lithium aluminium tetrahydride / tetrahydrofuran / -10 - 20 °C
6.1: triethylamine / dichloromethane / -10 - 20 °C
With
lithium aluminium tetrahydride; potassium tert-butylate; ammonia; water; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
