C₅₇H₆₈N₈O₁₅

Base Information

Chemical Name:C₅₇H₆₈N₈O₁₅
CAS No.:1428244-82-9
Molecular Formula:C₅₇H₆₈N₈O₁₅
Molecular Weight:1105.21
Hs Code.:

C<sub>57</sub>H<sub>68</sub>N<sub>8</sub>O<sub>15</sub>

Synonyms:C₅₇H₆₈N₈O₁₅

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Chemical Property of C₅₇H₆₈N₈O₁₅

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Technology Process of C₅₇H₆₈N₈O₁₅

There total 8 articles about C₅₇H₆₈N₈O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: C₂₂H₂₆N₂O₉

: 1428244-78-3
C₃₉H₄₇N₇O₉

: 1428244-82-9
C₅₇H₆₈N₈O₁₅

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 17h; Cooling with ice;
DOI:10.1021/ja400970n

Reference yield:

: 1263427-68-4
C₁₆H₂₈N₄O₆

: 1428244-82-9
C₅₇H₆₈N₈O₁₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16.5 h / 20 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

3.1: acetic acid / water / 16 h / 20 °C

3.2: 2 h / 20 °C

4.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 16 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C / Cooling with ice

7.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice

8.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 20 °C / Cooling with ice

With potassium hydrogencarbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja400970n

Reference yield:

: C₁₉H₃₃N₅O₇

: 1428244-82-9
C₅₇H₆₈N₈O₁₅

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 16 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C / Cooling with ice

4: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Cooling with ice

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 20 °C / Cooling with ice

With potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja400970n