Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate

Base Information

Chemical Name:Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate
CAS No.:86288-21-3
Molecular Formula:C₁₇H₂₀NO₆*Na
Molecular Weight:357.339
Hs Code.:

Synonyms:Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate

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Chemical Property of Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate

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Technology Process of Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate

There total 5 articles about Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84923-68-2
5-(benzyloxy)-2-methoxybenzoic acid

: 86288-21-3
Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / H₂SO₄ (concn) / 2-methyl-propan-2-ol; CH₂Cl₂ / 50 h / Ambient temperature

2: 91 percent / H₂ / Pd/C / ethanol / 2250.2 Torr

3: 1.) sodium methylate / 1.) methanol; 2.) DMF, room temp., 20h

4: 1N NaOH / dioxane / 4 h

With sodium hydroxide; sulfuric acid; hydrogen; sodium methylate; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/jo00164a010

Reference yield:

: 86272-63-1
tert-Butyl 5-(Benzyloxy)-2-methoxybenzoate

: 86288-21-3
Sodium 3-<<3-(tert-Butoxycarbonyl)-4-methoxyphenyl>-oxy>-1-pyrroline-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / Pd/C / ethanol / 2250.2 Torr

2: 1.) sodium methylate / 1.) methanol; 2.) DMF, room temp., 20h

3: 1N NaOH / dioxane / 4 h

With sodium hydroxide; hydrogen; sodium methylate; palladium on activated charcoal; In 1,4-dioxane; ethanol;
DOI:10.1021/jo00164a010