methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate

Base Information

Chemical Name:methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate
CAS No.:82555-63-3
Molecular Formula:C₁₈H₂₆O₂Si
Molecular Weight:302.489
Hs Code.:

Synonyms:methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate

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Chemical Property of methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate

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Technology Process of methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate

There total 1 articles about methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 14630-42-3
(3,3-dimethyl-1-butynyl)trimethylsilane

: 22979-35-7
Methyl phenyldiazoacetate

: 82555-63-3
methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate

Guidance literature:: at 130 ℃;
DOI:10.1021/ja00382a019

Reference yield: 55.0%

: 82555-63-3
methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate

: 82555-67-7
2-tert-butyl-1-phenyl-2-cyclopropene-1-carboxylic acid

Guidance literature:: With potassium hydroxide; In water;
DOI:10.1021/ja00382a019

Reference yield:

: 82555-63-3
methyl 2-tert-butyl-1-phenyl-3-(trimethylsilyl)-2-cyclopropene-1-carboxylate

: 82555-57-5
2-tert-butyl-1-phenyl-2-cyclopropene-1-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / potassium hydroxide / H₂O

2: oxalyl chloride

With potassium hydroxide; oxalyl dichloride; In water;
DOI:10.1021/ja00382a019