8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Base Information

Chemical Name:8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine
CAS No.:59469-04-4
Molecular Formula:C₁₉H₁₇ClFN₃
Molecular Weight:341.815
Hs Code.:

8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4<i>H</i>-benzo[<i>f</i>]imidazo[1,5-<i>a</i>][1,4]diazepine

Synonyms:8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

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Chemical Property of 8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Chemical Property:

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Technology Process of 8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

There total 11 articles about 8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59468-07-4
8-chloro-6-(2-fluorophenyl)-5,6-dihydro-1-methyl-6H-imidazo<1,5-a><1,4>benzodiazepine

: 59469-04-4
8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Guidance literature:: With potassium hydroxide; formaldehyd; In formic acid;

Reference yield:

: 7-chloro-1,3-dihydro-5-(2-fluorophenyl)-2-(1-nitromethylene)-2H-1,4-benzodiazepine 4-oxide

: 59469-04-4
8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 6 steps

1: aluminum nickel / tetrahydrofuran; methanol

2: PPA; acetic anhydride / methanol; dichloromethane; water

3: hydrogen / dichloromethane; water; acetic acid; Petroleum ether

4: manganese dioxide / toluene

5: zinc / dichloromethane; water; acetic acid

6: potassium hydroxide; formaldehyd / formic acid

With potassium hydroxide; formaldehyd; PPA; manganese dioxide; hydrogen; acetic anhydride; zinc; aluminum nickel; In tetrahydrofuran; methanol; formic acid; dichloromethane; water; acetic acid; toluene; Petroleum ether;

Reference yield:

: 59469-74-8
8-chloro-6-(2-fluorophenyl)-1-methyl-6H-imidazo<1,5-a><1,4>benzodiazepine

: 59469-04-4
8-chloro-6-(2-fluoro-phenyl)-1,5-dimethyl-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: N-methyl-acetamide; acetic acid; ethyl acetate

2: zinc / dichloromethane; water; acetic acid

3: potassium hydroxide; formaldehyd / formic acid

With potassium hydroxide; formaldehyd; zinc; In N-methyl-acetamide; formic acid; dichloromethane; water; acetic acid; ethyl acetate;