5-trimethylsilanylbenzene-1,2,3,4-tetracarboxylic acid tetra-tert-butyl ester

Base Information

Chemical Name:5-trimethylsilanylbenzene-1,2,3,4-tetracarboxylic acid tetra-tert-butyl ester
CAS No.:1610528-53-4
Molecular Formula:C₂₉H₄₆O₈Si
Molecular Weight:550.765
Hs Code.:

Synonyms:5-trimethylsilanylbenzene-1,2,3,4-tetracarboxylic acid tetra-tert-butyl ester

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Chemical Property of 5-trimethylsilanylbenzene-1,2,3,4-tetracarboxylic acid tetra-tert-butyl ester

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Technology Process of 5-trimethylsilanylbenzene-1,2,3,4-tetracarboxylic acid tetra-tert-butyl ester

There total 1 articles about 5-trimethylsilanylbenzene-1,2,3,4-tetracarboxylic acid tetra-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 66086-33-7
Di-tert-butyl acetylenedicarboxylate

: 1066-54-2
trimethylsilylacetylene

: 1610528-51-2
3,6-bis(trimethylsilanyl)phthalic acid di-tert-butyl ester

: 1610528-53-4
5-trimethylsilanylbenzene-1,2,3,4-tetracarboxylic acid tetra-tert-butyl ester

: 1610528-52-3
3,5-bis(trimethylsilanyl)-phthalic acid di-tert-butyl ester

Guidance literature:: With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; (R)-tol-BINAP; In dichloromethane; at 20 ℃; for 16h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/anie.201310336