(S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid

Base Information

Chemical Name:(S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid
CAS No.:935481-12-2
Molecular Formula:C₂₀H₃₁NO₄S₃
Molecular Weight:445.668
Hs Code.:

Synonyms:(S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid

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Chemical Property of (S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid

Chemical Property:

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Technology Process of (S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid

There total 7 articles about (S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141437-94-7
((S)-1-Mercaptomethyl-3-methylsulfanyl-propyl)-carbamic acid tert-butyl ester

: 147783-10-6,69734-01-6
(S)-BMPA

: 935481-12-2
(S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid

Guidance literature:: ((S)-1-Mercaptomethyl-3-methylsulfanyl-propyl)-carbamic acid tert-butyl ester; With metgoxycarbonylsulfenyl chloride; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;

(S)-BMPA; With triethylamine; In tetrahydrofuran; methanol; chloroform; at 20 ℃; for 1h;

Reference yield:

: 139429-04-2
Thioacetic acid S-((S)-2-tert-butoxycarbonylamino-4-methylsulfanyl-butyl) ester

: 935481-12-2
(S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; methanol

2: tetrahydrofuran; methanol / 0.5 h / 20 °C

3: triethylamine / dichloromethane / 1 h / 20 °C

With methanol; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm500602h

Reference yield:

: 247093-36-3
(S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl methanesulfonate

: 935481-12-2
(S)-2-benzyl-3-(((S)-2-(tert-butoxycarbonylamino)-4-(methylthio)butyl)disulfanyl)propanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide

2: sodium hydroxide; methanol

3: tetrahydrofuran; methanol / 0.5 h / 20 °C

4: triethylamine / dichloromethane / 1 h / 20 °C

With methanol; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm500602h