N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane

Base Information

Chemical Name:N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane
CAS No.:1384683-75-3
Molecular Formula:C₂₆H₂₆ClN₃O₄
Molecular Weight:479.963
Hs Code.:

Synonyms:N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane

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Chemical Property of N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane

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Technology Process of N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane

There total 2 articles about N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1384683-74-2
N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-TMS-propioloyl-1,4-diaminobutane

: 1384683-75-3
N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane

Guidance literature:: With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1039/c2cc31335a

Reference yield:

: C₁₀H₂₀N₂OSi

: 1384683-75-3
N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

2: tetrabutyl ammonium fluoride; water / tetrahydrofuran / 0.5 h / 20 °C

With tetrabutyl ammonium fluoride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2cc31335a

Reference yield: 79.0%

: 459-23-4,7304-35-0
4-fluorobenzaldoxime

: 1384683-75-3
N-2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetyl-N'-propioloyl-1,4-diaminobutane

: 1384683-66-2
C₃₃H₃₀ClFN₄O₅

Guidance literature:: With bis-[(trifluoroacetoxy)iodo]benzene; In methanol; water; N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1039/c2cc31335a