1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol

Base Information

• Chemical Name: 1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol
• CAS No.: 1023292-14-9
• Molecular Formula: C₂₁H₂₅FO₄S
• Molecular Weight: 392.492

Synonyms:1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol

Chemical Property of 1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol

Chemical Property:

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Technology Process of 1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol

There total 1 articles about 1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-anhydro-2-deoxy-2-fluoro-4-thio-D-arabinitol (878384-22-6) + p-methoxybenzyl chloride (824-94-2) → 1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol (1023292-14-9)

Guidance literature:

1,4-anhydro-2-deoxy-2-fluoro-4-thio-D-arabinitol; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; at 20 ℃; Further stages.;

DOI:10.1016/j.carres.2008.01.025

Reference yield: 70.0%

1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol (1023292-14-9) + 2,4-O-benzylidene-L-erythritol-1,3-cyclic sulfate (334024-20-3) → 1,2,4-trideoxy-2-fluoro-3,5-di-O-p-methoxybenzyl-1,4-[[(2S,3S)-2,4-O-benzylidene-3-(sulfooxy)butyl]episulfoniumylidene]-D-arabinitol inner salt

Guidance literature:

With potassium carbonate; In various solvent(s); at 68 ℃;

DOI:10.1016/j.carres.2008.01.025

Reference yield: 62.0%

1,4-anhydro-2-deoxy-2-fluoro-3,5-di-O-(p-methoxybenzyl)-4-thio-D-arabinitol (1023292-14-9) + 2,4-O-benzylidene-L-erythritol-1,3-cyclic sulfate (334024-20-3) → 1,4-dideoxy-1,2-ene-3,5-di-O-p-methoxybenzyl-1,4-[[(2S,3S)-2,4-O-benzylidene-3-(sulfooxy)butyl]episulfoniumylidene]-D-arabinitol inner salt

Guidance literature:

With potassium carbonate; In various solvent(s); at 70 ℃; for 20h;

DOI:10.1016/j.carres.2008.01.025

upstream raw materials:

1,4-anhydro-2-deoxy-2-fluoro-4-thio-D-arabinitol

p-methoxybenzyl chloride

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