Technology Process of C22H25N5O5S
There total 7 articles about C22H25N5O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H33N5O5S;
With
trifluoroacetic acid;
In
dichloromethane;
at 2 ℃;
for 20h;
With
sodium hydroxide; water;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 2h;
With
hydrogenchloride;
In
tetrahydrofuran; methanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 20 °C
2.1: hydrogenchloride / ethanol; isopropyl alcohol / 21 h / Heating / reflux
3.1: trifluoroacetic acid / dichloromethane / 20 h / 2 °C
3.2: 2 h / 20 °C
With
hydrogenchloride; hydrogen; trifluoroacetic acid;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / water; toluene / 1 h / 20 - 90 °C
2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 20 °C
3.1: hydrogenchloride / ethanol; isopropyl alcohol / 21 h / Heating / reflux
4.1: trifluoroacetic acid / dichloromethane / 20 h / 2 °C
4.2: 2 h / 20 °C
With
hydrogenchloride; sodium hydroxide; hydrogen; trifluoroacetic acid;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; water; isopropyl alcohol; toluene;