2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate

Base Information

Chemical Name:2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate
CAS No.:1382487-85-5
Molecular Formula:C₂₈H₃₀N₂O₂
Molecular Weight:426.558
Hs Code.:

Synonyms:2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate

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Chemical Property of 2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate

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Technology Process of 2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate

There total 3 articles about 2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1382487-84-4
2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenol

: 108-24-7
acetic anhydride

: 1382487-85-5
2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate

Guidance literature:: With pyridine; dmap; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2012.04.048

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1382487-85-5
2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

2: acetic acid / 4 h / Reflux

3: 160 °C / Neat (no solvent)

4: pyridine; dmap / 3 h / 20 °C

With pyridine; dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/j.bmc.2012.04.048

Reference yield:

: 90-01-7
salicylic alcohol

: 129226-09-1
2-<1-(4-isobutylphenyl)ethyl>-1H-benzimidazole

: 1382487-85-5
2-({2-[1-(4-isobutylphenyl)ethyl]-1H-benzimidazol-1-yl}methyl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 160 °C / Neat (no solvent)

2: pyridine; dmap / 3 h / 20 °C

With pyridine; dmap;
DOI:10.1016/j.bmc.2012.04.048