tris(2,6-diisopropylphenylimido)osmium

Base Information

Chemical Name:tris(2,6-diisopropylphenylimido)osmium
CAS No.:925216-59-7
Molecular Formula:C₃₆H₅₁N₃Os
Molecular Weight:716.021
Hs Code.:

Synonyms:tris(2,6-diisopropylphenylimido)osmium

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Chemical Property of tris(2,6-diisopropylphenylimido)osmium

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Technology Process of tris(2,6-diisopropylphenylimido)osmium

There total 4 articles about tris(2,6-diisopropylphenylimido)osmium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 20816-12-0
osmium(VIII) oxide

: 78923-65-6
N-trimethylsilyl-2,6-diisopropylaniline

: 925216-59-7
tris(2,6-diisopropylphenylimido)osmium

Guidance literature:: In neat (no solvent); OsO4 in neat NH(C6H3(CH(CH3)2)2)(Si(CH3)3) was heated at 100-120°C for2-3h; excess silylamine was removed at 120°C 6.6 Pa, extd. with hexane, concd. cooled to -20°C for 24h;

Reference yield: 50.0%

: 20816-12-0
osmium(VIII) oxide

: 28178-42-9
2,6-diisopropylphenyl isocyanate

: 925216-59-7
tris(2,6-diisopropylphenylimido)osmium

Guidance literature:: In n-heptane; a mixt. of OsO4 and 2,6-diisopropylphenyl isocyanate is refluxed in heptane under argon for 20 h;; crystn. upon cooling to ambient temp.; elem. anal.;;