3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate

Base Information

Chemical Name:3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate
CAS No.:912644-36-1
Molecular Formula:C₂₂H₂₂N₂O₈
Molecular Weight:442.425
Hs Code.:

Synonyms:3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate

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Chemical Property of 3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate

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Technology Process of 3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate

There total 1 articles about 3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 912644-39-4
C₁₂H₁₅NO₄

: 86255-43-8,56723-84-3
1,3-dimethoxy-5-(2-nitroethenyl)benzene

: 912644-21-4
3,5-bis(3,5-dimethoxyphenyl)-1H-pyrrole-2-methyl carboxylate

: 912644-36-1
3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate

Guidance literature:: C₁₂H₁₅NO₄; 1,3-dimethoxy-5-(2-nitroethenyl)benzene; With silver(I) acetate; triethylamine; In acetonitrile; for 5h;

With manganese(IV) oxide; In diethylene glycol dimethyl ether; for 48h; Reflux; Inert atmosphere;

Reference yield:

: 912644-36-1
3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate

: 912644-30-5
4-amino-3,5-bis(3,5-dimethoxyphenyl)-1H-pyrrole-2-methyl carboxylate

Guidance literature:: 3,5-bis(3,5-dimethoxyphenyl)-4-nitro-1H-pyrrole-2methyl carboxylate; With tin(II) chloride dihdyrate; In N,N-dimethyl-formamide; at 50 ℃; for 16h;

With sodium carbonate; acetic acid; In water; N,N-dimethyl-formamide;