2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

Base Information

Chemical Name:2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin
CAS No.:72163-46-3
Molecular Formula:C₃₅H₄₀N₄O₁₅
Molecular Weight:756.72
Hs Code.:

2',3'-dideoxy-2',3'-<N-(benzyloxycarbonyl)epimo>-3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

Synonyms:2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

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Chemical Property of 2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

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Technology Process of 2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

There total 6 articles about 2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 72163-45-2
C₄₂H₄₈N₄O₁₈S

: 72163-46-3
2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 25 ℃; for 22h;
DOI:10.1021/jm00175a009

Reference yield:

: 72163-44-1
3,2'-bis-1,6:6',4'-N,O-dicarbonyl-2'',3''-O-cyclohexylidene-3'-O-toluenesulfonyl-5''-O-(triphenylmethyl)ribostamycin

: 72163-46-3
2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / acetic acid / 12 h / 70 - 80 °C

2: 69 percent / NaH / dimethylformamide / 22 h / 25 °C

With sodium hydride; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00175a009

Reference yield:

: 72163-43-0
C₆₀H₆₄N₄O₁₆

: 72163-46-3
2',3'-dideoxy-2',3'--3-N-(benzyloxycarbonyl)-1,6:6',4'-N,O-dicarbonylribostamycin

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine / 48 h / 25 °C

2: 82 percent / acetic acid / 12 h / 70 - 80 °C

3: 69 percent / NaH / dimethylformamide / 22 h / 25 °C

With sodium hydride; In pyridine; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00175a009