N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine

Base Information

Chemical Name:N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine
CAS No.:1229621-60-6
Molecular Formula:C₂₁H₂₈N₄
Molecular Weight:336.48
Hs Code.:

Synonyms:N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine

There total 10 articles about N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1445-73-4
1-Methyl-4-piperidone

: 21241-08-7
2-methyl-5-{2-[1-(4-methylphenyl)hydrazinyl]ethyl}pyridine

: 1229621-60-6
N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine

Guidance literature:: In benzene; for 2h; Reflux; Molecular sieve;

Reference yield:

: 2-methyl-5-(2-[N-nitroso-(2-methylphenyl)amino]ethyl)pyridine

: 1229621-60-6
N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol; water / 0.5 h / 60 °C / Inert atmosphere

1.2: 12 h / 60 °C / Inert atmosphere

2.1: toluene / 24 h / 120 °C

With sodium hydroxide; In ethanol; water; toluene;

Reference yield:

: 36357-38-7
1-(6-methyl-pyridin-3-yl)-ethanone

: 1229621-60-6
N'-(1-methyl-piperidin-4-ylidene)-N-[2-(6-methyl-pyridin-3-yl)-ethyl]-N-p-tolyl-hydrazine

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfur / 7 h / 110 °C

2.1: sodium hydroxide; water / ethanol / 17 h / 80 °C

2.2: pH 2

3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 12 h / 20 °C

4.1: sodium tetrahydroborate; acetic acid / 1,4-dioxane / 3.5 h / 10 - 105 °C

5.1: hydrogenchloride / water / 30 °C

5.2: 1 h / 0 - 20 °C

5.3: 1 h

6.1: sodium hydroxide / ethanol; water / 0.5 h / 60 °C / Inert atmosphere

6.2: 12 h / 60 °C / Inert atmosphere

7.1: toluene / 24 h / 120 °C

With hydrogenchloride; sodium tetrahydroborate; water; benzotriazol-1-ol; sulfur; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; toluene;