[Os(η5-C5H2Me(SiMe3)2)(bipy)(PPh3)]OTf

Base Information

• Chemical Name: [Os(η5-C5H2Me(SiMe3)2)(bipy)(PPh3)]OTf
• CAS No.: 915725-18-7
• Molecular Formula: CF₃O₃S*C₄₀H₄₆N₂OsPSi₂
• Molecular Weight: 981.234

Synonyms:[Os(η5-C5H2Me(SiMe3)2)(bipy)(PPh3)]OTf

Chemical Property of [Os(η5-C5H2Me(SiMe3)2)(bipy)(PPh3)]OTf

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Technology Process of [Os(η5-C5H2Me(SiMe3)2)(bipy)(PPh3)]OTf

There total 1 articles about [Os(η5-C5H2Me(SiMe3)2)(bipy)(PPh3)]OTf which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

sodium tetrahydroborate (16940-66-2) + [Os(CC(SiMe3)=C(Me)C(SiMe3)=CH)(bipy)(PPh3)2](OTf)2 → [Os(η5-C5H2Me(SiMe3)2)(bipy)(PPh3)]OTf (915725-18-7)

Guidance literature:

In tetrahydrofuran; under N2 atm. mixt. Os complex and NaBH4 in THF was stirred for 4 h; soln. was filtered and evapd. to dryness in vacuo, residue was dissolvedin CH2Cl2, Et2O was added, ppt. was filtered, washed with hexane and dr ied in vacuo; elem. anal.;

DOI:10.1021/ja064570w

upstream raw materials:

sodium tetrahydroborate

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