(3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester

Base Information

• Chemical Name: (3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester
• CAS No.: 909914-51-8
• Molecular Formula: C₂₆H₃₇NO₃
• Molecular Weight: 411.585

Synonyms:(3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester

Chemical Property of (3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester

Chemical Property:

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Technology Process of (3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester

There total 2 articles about (3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(3S,5R,7aR,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester → (3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester (909914-51-8)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 20h;

Reference yield:

(2S,12E)-2-(diphenylmethylene)amino-5,11-dioxo-12-nonadecenoic acid benzyl ester → (3S,5R,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester (909914-51-8) + (3S,5S,7aS,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester + (3S,5R,7aR,11aS)-5-hexyloctahydro-pyrrolo-1H-[2,1-j]quinolin-7-one-3-carboxyxlic acid benzyl ester

Guidance literature:

With camphor-10-sulfonic acid; magnesium chloride; In 1,2-dichloro-ethane; at 50 ℃; for 12h; Further Variations:; Reagents; Product distribution;

DOI:10.1002/anie.200601722

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