C₁₈H₂₆N₂O₇

Base Information

Chemical Name:C₁₈H₂₆N₂O₇
CAS No.:190248-43-2
Molecular Formula:C₁₈H₂₆N₂O₇
Molecular Weight:382.414
Hs Code.:

C<sub>18</sub>H<sub>26</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₁₈H₂₆N₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₆N₂O₇

Chemical Property:

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Technology Process of C₁₈H₂₆N₂O₇

There total 1 articles about C₁₈H₂₆N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 2476-35-9
5-bromo-2-methoxybenzoic acid

: 190248-43-2
C₁₈H₂₆N₂O₇

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) THF, hexanes, -78 deg C, 15 min, 2) THF, hexanes, -78 deg C, 5 min; -78 deg C -> 25 deg C, 20 min;
DOI:10.1021/ja963843s

Reference yield:

: 190248-43-2
C₁₈H₂₆N₂O₇

: 5-Hydrazino-2-methoxy-N-methyl-benzamide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1-hydroxybenzotriazole hydrate, 1-ethyl-3-(3'-dimethylaminopropyl)carbodiimide hydrochloride / 1) MeOH, 24 min, 2) MeOH, 2 h

2: HCl / methanol / 26 h

With hydrogenchloride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol;
DOI:10.1021/ja963843s

Reference yield:

: 190248-43-2
C₁₈H₂₆N₂O₇

: 5-{N'-[5-(3,3-Diethyl-ureido)-2-methoxy-benzoyl]-hydrazino}-2-methoxy-N-methyl-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 1-hydroxybenzotriazole hydrate, 1-ethyl-3-(3'-dimethylaminopropyl)carbodiimide hydrochloride / 1) MeOH, 24 min, 2) MeOH, 2 h

2: HCl / methanol / 26 h

3: 82 percent / EDC*HCl, HOBt*H₂O, Et₃N / methanol / 4 h

With hydrogenchloride; benzotriazol-1-ol; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol;
DOI:10.1021/ja963843s