benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate

Base Information

Chemical Name:benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate
CAS No.:1612873-43-4
Molecular Formula:C₂₈H₃₃NO₅Si
Molecular Weight:491.659
Hs Code.:

Synonyms:benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate

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Technology Process of benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate

There total 2 articles about benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 621-84-1
O-benzyl carbamate

: 1612873-29-6
(E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)prop-2-en-1-ol

: 1612873-43-4
benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate

Guidance literature:: With perrhenic acid anhydride; In dichloromethane; at 20 - 45 ℃; Inert atmosphere;
DOI:10.1002/chem.201400104

Reference yield:

: 10079-74-0
1-(3,4,5-trimethoxyphenyl)prop-2-yn-1-ol

: 766-77-8
Dimethylphenylsilane

: 1612873-43-4
benzyl (E)-1-(3,4,5-trimethoxyphenyl)-3-(dimethyl(phenyl)silyl)allylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: XPhos; platinum(II) chloride / tetrahydrofuran / 50 °C / Inert atmosphere

2: perrhenic acid anhydride / dichloromethane / 20 - 45 °C / Inert atmosphere

With perrhenic acid anhydride; platinum(II) chloride; XPhos; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201400104