4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride

Base Information

Chemical Name:4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride
CAS No.:1027973-80-3
Molecular Formula:C₁₃H₁₃Cl₂N₃O
Molecular Weight:298.172
Hs Code.:

4-chloro-3-cyclopentyl-1-methyl-1<i>H</i>-pyrazolo[3,4-<i>b</i>]pyridine-5-carbonyl chloride

Synonyms:4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride

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Technology Process of 4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride

There total 1 articles about 4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95882-33-0
3-cyclopentyl-3-oxopropanenitrile

: 1027973-80-3
4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N / ethanol / Heating

2: 120 °C

3: POCl₃ / 120 °C

4: aq. KOH / 1,2-dimethoxy-ethane / 20 °C

5: SOCl₂ / 80 °C

With potassium hydroxide; thionyl chloride; triethylamine; trichlorophosphate; In 1,2-dimethoxyethane; ethanol; 2: Michael addition;
DOI:10.1248/cpb.52.1098

Reference yield:

: 1027973-80-3
4-chloro-3-cyclopentyl-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carbonyl chloride

: 3-cyclopentyl-4-[(3-methoxyphenyl)amino]-1-methyl-1H-pyrazolo[3,4-b]pyridine-5-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NH₃ / tetrahydrofuran / 0 °C

2: 75 percent / dioxane / Heating

With ammonium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1248/cpb.52.1098