5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside

Base Information

Chemical Name:5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside
CAS No.:160243-06-1
Molecular Formula:C₃₅H₄₃NO₈
Molecular Weight:605.728
Hs Code.:

Synonyms:5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside

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Chemical Property of 5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside

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Technology Process of 5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside

There total 2 articles about 5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87905-98-4
5-<(benzyloxycarbonyl)amino>pentanol

: ethyl 3-O-acetyl-2,4-di-O-benzyl-1-deoxy-1-thio-L-fucopyranoside

: 160243-06-1
5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; In dichloromethane; at -30 ℃; for 0.75h; Yield given;
DOI:10.1016/0008-6215(94)84179-9

Reference yield:

: 1,3-di-O-acetyl-2,4-di-O-benzyl-L-fucopyranoside

: 160243-06-1
5-(benzyloxycarbonylamino)pentyl 3-O-acetyl-2,4-di-O-benzyl-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃*Et₂O / CH₂Cl₂ / 0.5 h / Ambient temperature

2: CF₃SO₃H,, mol. sieves 3A, N-iodosuccinimide / CH₂Cl₂ / 0.75 h / -30 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/0008-6215(94)84179-9