Technology Process of C26H23N5
There total 13 articles about C26H23N5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; methanol;
In
dichloromethane;
at 0 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: thionyl chloride / dichloromethane / 2.33 h / 0 - 20 °C
1.2: pH > 7 / Saturated solution
2.1: N,N-dimethyl-formamide / 20 - 80 °C
3.1: 6 h / 120 °C
4.1: hydrazine monohydrobromide / ethanol; water / 5 h / 110 °C
4.2: Saturated solution
5.1: acetic acid / ethanol / 5 h / 50 °C
6.1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 150 °C / Inert atmosphere; Microwave irradiation
7.1: hydrogen / platinum(IV) oxide; 5%-palladium/activated carbon / methanol; dichloromethane
8.1: hydrogenchloride; methanol / dichloromethane / 0 - 20 °C
With
hydrogenchloride; methanol; thionyl chloride; hydrazine monohydrobromide; hydrogen; potassium carbonate; acetic acid;
platinum(IV) oxide; tetrakis(triphenylphosphine) palladium(0); 5%-palladium/activated carbon;
In
1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: methanol; sodium tetrahydroborate / 1.33 h / 0 - 20 °C
2.1: thionyl chloride / dichloromethane / 2.33 h / 0 - 20 °C
2.2: pH > 7 / Saturated solution
3.1: N,N-dimethyl-formamide / 20 - 80 °C
4.1: 6 h / 120 °C
5.1: hydrazine monohydrobromide / ethanol; water / 5 h / 110 °C
5.2: Saturated solution
6.1: acetic acid / ethanol / 5 h / 50 °C
7.1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 150 °C / Inert atmosphere; Microwave irradiation
8.1: hydrogen / platinum(IV) oxide; 5%-palladium/activated carbon / methanol; dichloromethane
9.1: hydrogenchloride; methanol / dichloromethane / 0 - 20 °C
With
hydrogenchloride; methanol; sodium tetrahydroborate; thionyl chloride; hydrazine monohydrobromide; hydrogen; potassium carbonate; acetic acid;
platinum(IV) oxide; tetrakis(triphenylphosphine) palladium(0); 5%-palladium/activated carbon;
In
1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;