2-Piperidinoneoxime

Base Information

• Chemical Name: 2-Piperidinoneoxime
• CAS No.: 4515-19-9
• Molecular Formula: C₅H₁₀N₂O
• Molecular Weight: 114.147
• Hs Code.: 2933790090
• Mol file: 4515-19-9.mol

Synonyms:2-Piperidinone,oxime (9CI); 2-Piperidone, oxime (6CI,7CI,8CI)

Chemical Property of 2-Piperidinoneoxime

Chemical Property:

• PSA: 44.62000
• LogP: 0.37410

Purity/Quality:

98%Min ^*data from raw suppliers

2-PIPERIDINONEOXIME 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Piperidinoneoxime

There total 3 articles about 2-Piperidinoneoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1-nitroso-piperidine-2-carboxylic acid (4515-18-8,30310-81-7) → 2-piperidonoxime (4515-19-9)

Guidance literature:

In diethyl ether; for 2h; Ambient temperature; Irradiation;

Reference yield:

piperidine-2-thione (13070-01-4) → piperidin-2-one oxime (4515-19-9)

Guidance literature:

With methanol; hydroxylamine hydrochloride; sodium hydrogencarbonate;

Reference yield:

→ piperidin-2-one oxime (4515-19-9)

Guidance literature:

N-Nitroso-piperidin in wss. Salzsaeure, Photolyse;

DOI:10.1139/v67-010

upstream raw materials:

piperidine-2-thione

1-nitroso-piperidine-2-carboxylic acid

Downstream raw materials:

1,3-diazepan-2-one

Refernces

• 1、 Chow, Yuan L.,Horning, Douglas P.,Polo, Joel. "Photochemistry of N-nitroso-N-alkyl amino acids: a facile oxidative decarboxylation". . p. 2477 - 2483. Retrieved 2007/10/02.