ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate

Base Information

Chemical Name:ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate
CAS No.:1453422-08-6
Molecular Formula:C₂₄H₂₃N₃O₂
Molecular Weight:385.466
Hs Code.:

Synonyms:ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate

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Chemical Property of ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate

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Technology Process of ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate

There total 4 articles about ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 68765-57-1
ethyl 3-amino-4-(phenylamino)benzoate

: 100-10-7
4-dimethylamino-benzaldehyde

: 1453422-08-6
ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate

Guidance literature:: With sodium metabisulfite; In water; at 20 ℃; for 2h;
DOI:10.1002/ardp.201500337

Reference yield:

: 367-80-6
ethyl 4-fluoro-3-nitrobenzoate

: 1453422-08-6
ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 1 h / 20 °C

2: ammonium formate; palladium 10% on activated carbon / ethanol / 20 °C

3: sodium meta bi sulfate / water / 2 h / 20 °C / Green chemistry

With sodium meta bi sulfate; palladium 10% on activated carbon; ammonium formate; In ethanol; water;
DOI:10.1016/j.ejmech.2014.06.060

Reference yield:

: 453-71-4
3-nitro-4-fluorobenzoic acid

: 1453422-08-6
ethyl 2-(4-(dimethylamino)phenyl)-1-phenyl-1H-benzo[d]-imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 6 h / Reflux

2: ethanol / 1 h / 20 °C

3: ammonium formate; palladium 10% on activated carbon / ethanol / 20 °C

4: sodium meta bi sulfate / water / 2 h / 20 °C / Green chemistry

With sodium meta bi sulfate; sulfuric acid; palladium 10% on activated carbon; ammonium formate; In ethanol; water;
DOI:10.1016/j.ejmech.2014.06.060