2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt

Base Information

Chemical Name:2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt
CAS No.:1234700-85-6
Molecular Formula:C₃₇H₄₂NO₂*Li
Molecular Weight:539.687
Hs Code.:

Synonyms:2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt

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Chemical Property of 2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt

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Technology Process of 2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt

There total 1 articles about 2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1234700-75-4
2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldimine

: 1234700-85-6
2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt

Guidance literature:: With trimethylsilylmethyllithium; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/om100251j

Reference yield: 89.0%

: trans-chloro(methyl)bis(trimethylphosphane)nickel(II)

: 1234700-85-6
2-(methoxydiphenylmethyl)-4-tert-butyl-[6-(2,6-diisopropylphenyl)]salicylaldiminate lithium salt

: 1234700-88-9
(2-(methoxydiphenylmethyl)-4-tert-butyl-6-[2,6-diisopropylphenyl]salicylaldiminato-κ2N,O)methyl(trimethylphosphine)nickel(II)

Guidance literature:: In benzene; (inert atm.); addn. of benzene soln. of lithiumm salt to benzene soln. of nickel compd. at room temp., stirring for 2 d at room temp.; cannula filtration, evapn., washing with pentane, elem. anal.;
DOI:10.1021/om100251j