13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

Base Information

Chemical Name:13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid
CAS No.:877291-09-3
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

Synonyms:13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

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Chemical Property of 13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

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Technology Process of 13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

There total 9 articles about 13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 877291-15-1
13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid, dimethyl ester

: 877291-09-3
13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

Guidance literature:: With methanol; tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 1670-82-2,261352-47-0
Indole-6-carboxylic acid

: 877291-09-3
13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

Guidance literature:: Multi-step reaction with 6 steps

1: diethyl ether / 1 h / -15 °C

2: triethylsilane; trifluoroacetic acid / dichloromethane / 12 h / 10 - 20 °C

3: pyridinium hydrobromide perbromide / tetrahydrofuran; chloroform / 2 - 2.66 h / 0 - 20 °C

4: sodium carbonate; lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 3 h / 100 °C

5: caesium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C

6: methanol; tetra(n-butyl)ammonium hydroxide / tetrahydrofuran / 20 °C

With methanol; triethylsilane; tetra(n-butyl)ammonium hydroxide; sodium carbonate; caesium carbonate; pyridinium hydrobromide perbromide; trifluoroacetic acid; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 877291-09-3
13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane / 12 h / 10 - 20 °C

2: pyridinium hydrobromide perbromide / tetrahydrofuran; chloroform / 2 - 2.66 h / 0 - 20 °C

3: sodium carbonate; lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 3 h / 100 °C

4: caesium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C

5: methanol; tetra(n-butyl)ammonium hydroxide / tetrahydrofuran / 20 °C

With methanol; triethylsilane; tetra(n-butyl)ammonium hydroxide; sodium carbonate; caesium carbonate; pyridinium hydrobromide perbromide; trifluoroacetic acid; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene;