4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine

Base Information

Chemical Name:4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine
CAS No.:1617505-49-3
Molecular Formula:C₄₇H₃₈ClN₇O₂
Molecular Weight:768.317
Hs Code.:

Synonyms:4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine

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Chemical Property of 4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine

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Technology Process of 4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine

There total 4 articles about 4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.7%

: 1617505-48-2
4,4’-dimethyl-4”-(4-(4,6-dichloro-1,3,5-triazin-2-ylamino)styryl)triphenylamine

: 69940-76-7
1-(2-aminoethylamino)anthracene-9,10-dione

: 1617505-49-3
4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine

Guidance literature:: In tetrahydrofuran; at 40 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c4tc00860j

Reference yield:

: 42906-19-4
4-[N,N-di(p-tolyl)amino]benzaldehyde

: 1617505-49-3
4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 2 h / 80 °C / Inert atmosphere

2.1: tin(II) chloride dihdyrate / ethanol / 8 h / 90 °C / Inert atmosphere

3.1: acetone / 0 - 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 12 h / 40 °C / Inert atmosphere

With tin(II) chloride dihdyrate; sodium hydride; In tetrahydrofuran; ethanol; acetone;
DOI:10.1039/c4tc00860j

Reference yield:

: 2767-70-6
(p-nitrobenzyl)triphenylphosphonium bromide

: 1617505-49-3
4,4'-dimethyl-4''-{4-[4-chloro-6-(2-(9,10-dioxoanthracen-1-ylamino)ethylamino)-1,3,5-triazin-2-ylamino]styryl}triphenylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 2 h / 80 °C / Inert atmosphere

2.1: tin(II) chloride dihdyrate / ethanol / 8 h / 90 °C / Inert atmosphere

3.1: acetone / 0 - 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 12 h / 40 °C / Inert atmosphere

With tin(II) chloride dihdyrate; sodium hydride; In tetrahydrofuran; ethanol; acetone;
DOI:10.1039/c4tc00860j