6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene

Base Information

Chemical Name:6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene
CAS No.:1422273-19-5
Molecular Formula:C₆₂H₁₀₆O₃S₃Sn
Molecular Weight:1114.43
Hs Code.:

Synonyms:6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene

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Chemical Property of 6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene

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Technology Process of 6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene

There total 2 articles about 6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187207-24-4
2-(3,4,5-tris-n-dodecyloxyphenyl)dithieno[3,2-b:2',3'-d]thiophene

: 1461-22-9
tributyltin chloride

: 1422273-19-5
6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene

Guidance literature:: 2-(3,4,5-tris-n-dodecyloxyphenyl)dithieno[3,2-b:2',3'-d]thiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h;

tributyltin chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1016/j.tet.2013.01.009

Reference yield:

: tri-n-butyl(dithieno[3,2-b:2',3'-d]thiophen-2-yl)stannane

: 1422273-19-5
6-[3,4,5-tris(dodecyloxy)phenyl]-2-tributylstannyl dithieno[3,2-b:2',3'-a]thiophene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / 110 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 - 20 °C

2.2: -78 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; In tetrahydrofuran; hexane; toluene;
DOI:10.1016/j.tet.2013.01.009