6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid

Base Information

• Chemical Name: 6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid
• CAS No.: 106115-80-4
• Molecular Formula: C₂₇H₂₇BrN₃O₈P
• Molecular Weight: 634.389

Synonyms:6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid

Chemical Property of 6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid

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Technology Process of 6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid

There total 1 articles about 6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1,6-Di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α,β-D-glucopyranose → 6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid (106115-80-4)

Guidance literature:

With titanium(IV) bromide; In dichloromethane; ethyl acetate; for 20h; Ambient temperature;

Reference yield: 96.0%

6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid (106115-80-4) + benzyl alcohol (100-51-6,185532-71-2) → Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid (106115-89-3)

Guidance literature:

With silver silicate; 4 A molecular sieve; In dichloromethane; at -20 ℃; for 3h;

Reference yield: 70.0%

Benzyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid (106115-82-6) + 6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid (106115-80-4) → Benzyl-6-O-<6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosyl>-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid (106115-92-8)

Guidance literature:

With silver silicate; 4 A molecular sieve; In dichloromethane; at -20 ℃; for 4h;

Downstream raw materials:

Benzyl-6-O-<6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosyl>-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid

Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

Benzyl-6-O-<6-O-acetyl-2-amino-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosyl>-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

Benzyl-6-O-acetyl-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-2-(tetradecanoylamino)-β-D-glucopyranosid

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