3-(dimethylamino)-2-phenoxypropanoic acid

Base Information

Chemical Name:3-(dimethylamino)-2-phenoxypropanoic acid
CAS No.:2132-43-6
Molecular Formula:C₁₁H₁₅NO₃
Molecular Weight:209.245
Hs Code.:

Synonyms:3-(dimethylamino)-2-phenoxypropanoic acid

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Chemical Property of 3-(dimethylamino)-2-phenoxypropanoic acid

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Technology Process of 3-(dimethylamino)-2-phenoxypropanoic acid

There total 3 articles about 3-(dimethylamino)-2-phenoxypropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 132291-69-1
ethyl 3-(dimethylamino)-2-phenoxypropanoate

: 2132-43-6
3-(dimethylamino)-2-phenoxypropanoic acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: ethyl 3-(benzyloxy)-2-phenoxypropanoate

: 2132-43-6
3-(dimethylamino)-2-phenoxypropanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 20% palladium hydroxide-activated charcoal; hydrogen / ethanol; water / 2 h / 20 °C

2.1: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 20 °C

With 20% palladium hydroxide-activated charcoal; water; hydrogen; Dess-Martin periodane; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water;