N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide
• CAS No.: 118158-10-4
• Molecular Formula: C₁₆H₁₈N₂O₄S
• Molecular Weight: 334.396
• Mol file: 118158-10-4.mol

Synonyms:N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Chemical Property of N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide

There total 1 articles about N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,4-Dimethoxybenzaldehyde (613-45-6) + toluene-4-sulfonic acid hydrazide (1576-35-8) → N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide (118158-10-4)

Guidance literature:

With polystyrene sulfonic acid; In water; at 100 ℃; for 0.0833333h; Wavelength; Reagent/catalyst; Solvent; Temperature; Microwave irradiation; Green chemistry;

DOI:10.1007/s00044-016-1543-9

Reference yield: 80.0%

dimedone (126-81-8) + N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide (118158-10-4) → C25H32O6 (139484-05-2)

Guidance literature:

In toluene; at 110 ℃; for 2h;

DOI:10.1016/j.tetlet.2017.02.001

Reference yield: 75.0%

1-(quinolin-8-yl)ethan-1-one (56234-20-9) + N'-(2,4-dimethoxybenzylidene)-4-methylbenzenesulfonohydrazide (118158-10-4) → C20H17NO3

Guidance literature:

With Wilkinson's catalyst; caesium carbonate; silver(l) oxide; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 48h; Inert atmosphere;

DOI:10.1055/s-0033-1339316

upstream raw materials:

2,4-Dimethoxybenzaldehyde

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

3-phenyl-6-(2,4-dimethoxyphenyl)-2.4-dioxo-3-azabicyclo<3.1.0>hexane

3-(2,4-dimethoxyphenyl)-7-(trifluoromethyl)-1H-indazole

C₂₅H₃₂O₆