(+)-hyosamine

Base Information

Chemical Name:(+)-hyosamine
CAS No.:31282-05-0
Molecular Formula:C₇H₁₆N₂O₃
Molecular Weight:176.216
Hs Code.:

Synonyms:(+)-hyosamine

Suppliers and Price of (+)-hyosamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-hyosamine

Chemical Property:

Purity/Quality:

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Technology Process of (+)-hyosamine

There total 7 articles about (+)-hyosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1L-(1,3/2,4,6)-6-azido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

: 31282-05-0
(+)-hyosamine

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / p-toluenesulfonic acid monohydrate / dioxane / 1 h / 25 °C

2: AcOH, 1,4-cyclohexadiene / 10percent Pd/C / methanol / 45 °C

3: 0.5 h

4: LiAlH₄ / dioxane / 1.5 h / Heating

5: 90percent trifluoroacetic acid / methanol / Ambient temperature

With lithium aluminium tetrahydride; cyclohexa-1,4-diene; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid; palladium on activated charcoal; In 1,4-dioxane; methanol;
DOI:10.1139/v91-231

Reference yield:

: 1L-(1,3/2,4,6)-6-azido-1,2-O-isopropylidene-4-nitro-3-O-(tetrahydropyran-2-yl)-1,2,3-cyclohexanetriol

: 31282-05-0
(+)-hyosamine

Guidance literature:: Multi-step reaction with 4 steps

1: AcOH, 1,4-cyclohexadiene / 10percent Pd/C / methanol / 45 °C

2: 0.5 h

3: LiAlH₄ / dioxane / 1.5 h / Heating

4: 90percent trifluoroacetic acid / methanol / Ambient temperature

With lithium aluminium tetrahydride; cyclohexa-1,4-diene; acetic acid; trifluoroacetic acid; palladium on activated charcoal; In 1,4-dioxane; methanol;
DOI:10.1139/v91-231