Technology Process of C11H15FO2S
There total 3 articles about C11H15FO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium fluoride;
In
acetone;
Reflux;
DOI:10.1021/jm301205j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tert.-butyl lithium / diethyl ether; pentane; hexane / 0.17 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: ammonium fluoride / acetone / Reflux
With
ammonium fluoride; tert.-butyl lithium;
In
diethyl ether; hexane; acetone; pentane;
DOI:10.1021/jm301205j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triphenylphosphine; 1H-imidazole; iodine / acetonitrile; diethyl ether / 0 - 20 °C / Inert atmosphere
2.1: tert.-butyl lithium / diethyl ether; pentane; hexane / 0.17 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 °C / Inert atmosphere
3.1: ammonium fluoride / acetone / Reflux
With
1H-imidazole; ammonium fluoride; iodine; tert.-butyl lithium; triphenylphosphine;
In
diethyl ether; hexane; acetone; acetonitrile; pentane;
DOI:10.1021/jm301205j