2-(3-chlorophenoxy)-N-[(Z)-1-(3,4-dimethoxyphenyl)ethylideneamino]acetamide

Base Information

Chemical Name:2-(3-chlorophenoxy)-N-[(Z)-1-(3,4-dimethoxyphenyl)ethylideneamino]acetamide
CAS No.:5567-29-3
Molecular Formula:C₁₂H₉BrO₂
Molecular Weight:265.106
Hs Code.:
DSSTox Substance ID:DTXSID10416956

Synonyms:5567-29-3;2-(3-chlorophenoxy)-N-[(Z)-1-(3,4-dimethoxyphenyl)ethylideneamino]acetamide;AC1NSWUN;DTXSID10416956;CCG-11931;BIM-0024861.P001;SR-01000213726;SR-01000213726-1

Suppliers and Price of 2-(3-chlorophenoxy)-N-[(Z)-1-(3,4-dimethoxyphenyl)ethylideneamino]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(3-chlorophenoxy)-N-[(Z)-1-(3,4-dimethoxyphenyl)ethylideneamino]acetamide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.21g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:362.1033348
Heavy Atom Count:25
Complexity:460

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NNC(=O)COC1=CC(=CC=C1)Cl)C2=CC(=C(C=C2)OC)OC
Isomeric SMILES:C/C(=N/NC(=O)COC1=CC(=CC=C1)Cl)/C2=CC(=C(C=C2)OC)OC

Technology Process of 2-(3-chlorophenoxy)-N-[(Z)-1-(3,4-dimethoxyphenyl)ethylideneamino]acetamide

There total 4 articles about 2-(3-chlorophenoxy)-N-[(Z)-1-(3,4-dimethoxyphenyl)ethylideneamino]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉H₇ClZn

: 5567-29-3
3-bromo-6-p-tolyl-pyran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Pd(PPh₃)4 / tetrahydrofuran / 0 - 20 °C

2: aq. LiOH / tetrahydrofuran / 20 °C

3: trans-di(μ-acetato)-bis<(di-o-tolylphosphino)benzyl>dipalladium(II) / toluene / 110 °C

With lithium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4039(98)00322-0

Reference yield:

: 208194-63-2
(E)-2-Bromo-5-p-tolyl-pent-2-en-4-ynoic acid ethyl ester

: 5567-29-3
3-bromo-6-p-tolyl-pyran-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: aq. LiOH / tetrahydrofuran / 20 °C

2: trans-di(μ-acetato)-bis<(di-o-tolylphosphino)benzyl>dipalladium(II) / toluene / 110 °C

With lithium hydroxide; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4039(98)00322-0

Reference yield:

: (E)-2-Bromo-5-p-tolyl-pent-2-en-4-ynoic acid

: 5567-29-3
3-bromo-6-p-tolyl-pyran-2-one

: 208194-67-6
3-Bromo-5-[1-p-tolyl-meth-(Z)-ylidene]-5H-furan-2-one

Guidance literature:: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); In toluene; at 110 ℃; Yield given;
DOI:10.1016/S0040-4039(98)00322-0