2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline

Base Information

• Chemical Name: 2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline
• CAS No.: 1244737-63-0
• Molecular Formula: C₂₈H₃₆N₂O₅
• Molecular Weight: 480.604

Synonyms:2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline

Chemical Property of 2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of 2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline

There total 1 articles about 2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

6,7-diethoxy-3,4-dihydroisoquinoline (53009-11-3) + Cyclohexyl isocyanide (931-53-3) + benzyl chloroformate (501-53-1,94274-21-2) → 2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline (1244737-63-0)

Guidance literature:

6,7-diethoxy-3,4-dihydroisoquinoline; Cyclohexyl isocyanide; benzyl chloroformate; In chloroform; at 20 ℃;

With water; In chloroform; at 20 ℃; for 0.5h;

DOI:10.1080/00397910903277920

Reference yield: 83.0%

2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline (1244737-63-0) → N-cyclohexyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline-1-carboxamide hydrobromide (1244737-76-5)

Guidance literature:

With hydrogen bromide; acetic acid;

DOI:10.1080/00397910903277920

Reference yield: 66.0%

2-benzyloxycarbonyl-1-cyclohexylcarbamoyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline (1244737-63-0) → N-cyclohexyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline-1-carboxamide (1244737-87-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃;

DOI:10.1080/00397910903277920

upstream raw materials:

6,7-diethoxy-3,4-dihydroisoquinoline

Cyclohexyl isocyanide

benzyl chloroformate

Downstream raw materials:

N-cyclohexyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline-1-carboxamide hydrobromide

N-cyclohexyl-6,7-diethoxy-1,2,3,4-tetrahydroisoquinoline-1-carboxamide

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