Technology Process of C22H25ClN4O5
There total 4 articles about C22H25ClN4O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2-chloro-1,3-dimethyl imidazolium chloride; triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C
2: nickel(II) chloride hexahydrate; sodium tetrahydroborate / dichloromethane; methanol
3: ethanol / 15 h / 20 °C
4: 2-chloro-1,3-dimethyl imidazolium chloride; triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C
With
sodium tetrahydroborate; 2-chloro-1,3-dimethyl imidazolium chloride; nickel(II) chloride hexahydrate; potassium carbonate; triethylamine;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / dichloromethane; methanol
2: ethanol / 15 h / 20 °C
3: 2-chloro-1,3-dimethyl imidazolium chloride; triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C
With
sodium tetrahydroborate; 2-chloro-1,3-dimethyl imidazolium chloride; nickel(II) chloride hexahydrate; triethylamine;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;