3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester

Base Information

Chemical Name:3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester
CAS No.:95852-63-4
Molecular Formula:C₃₁H₃₇N₂O₈P
Molecular Weight:596.617
Hs Code.:

Synonyms:3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester

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Chemical Property of 3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester

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Technology Process of 3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester

There total 1 articles about 3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 77526-73-9
(1-Amino-2-phenylethyl)phosphonsaeure-diethylester

: 29880-21-5
β-benzyl N-benzyloxycarbonyl-DL-aspartate

: 95852-63-4
3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; In chloroform; for 12h; Ambient temperature;
DOI:10.1002/jps.2600731252

Reference yield:

: 95852-63-4
3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester

: 95852-64-5
3-Amino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 760 Torr; Ambient temperature;
DOI:10.1002/jps.2600731252

Reference yield:

: 95852-63-4
3-Benzyloxycarbonylamino-N-[1-(diethoxy-phosphoryl)-2-phenyl-ethyl]-succinamic acid benzyl ester

: 3-Amino-N-(2-phenyl-1-phosphono-ethyl)-succinamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd(C) / methanol / 760 Torr / Ambient temperature

2: 50 percent / 48percent HBr / acetic acid / 0.33 h / 60 °C

With hydrogen bromide; hydrogen; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1002/jps.2600731252