4-MethyluMbelliferyl 2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylMethylene-α-D-galactopyranoside

Base Information

Chemical Name:4-MethyluMbelliferyl 2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylMethylene-α-D-galactopyranoside
CAS No.:1147438-61-6
Molecular Formula:C₃₇H₃₉N₃O₁₆
Molecular Weight:781.727
Hs Code.:
Mol file:1147438-61-6.mol

Synonyms:4-methylumbelliferyl 2-azido-4,6-O-benzylidene-2-deoxy-3-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranoside

Suppliers and Price of 4-MethyluMbelliferyl 2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylMethylene-α-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Methylumbelliferyl2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylmethylene-α-D-galactopyranoside
25mg
$ 675.00

TRC
4-Methylumbelliferyl2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylmethylene-α-D-galactopyranoside
5mg
$ 150.00

Medical Isotopes, Inc.
4-Methylumbelliferyl2-azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4-6-O-benzylidene-α-D-galactopyranoside
10 mg
$ 896.00

Medical Isotopes, Inc.
4-Methylumbelliferyl2-azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4-6-O-benzylidene-α-D-galactopyranoside
2 mg
$ 450.00

AK Scientific
[(2R,3S,4S,5R,6R)-6-[[(2S,4Ar,6R,7R,8R,8aR)-7-azido-6-(4-methyl-2-oxochromen-7-yl)oxy-2-phenyl-4,4a,6,7,8,8a-hexahydropyrano[3,2-d][1,3]dioxin-8-yl]oxy]-3,4,5-triacetyloxyoxan-2-yl]methylacetate
2mg
$ 252.00

Total 1 raw suppliers

Chemical Property of 4-MethyluMbelliferyl 2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylMethylene-α-D-galactopyranoside

Chemical Property:

Melting Point:124-126°C
Storage Temp.:Refrigerator
Solubility.:Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

4-Methylumbelliferyl2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylmethylene-α-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 4-Methylumbelliferyl 2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylmethylene-α-D-galactopyranoside (cas# 1147438-61-6) is a compound useful in organic synthesis.

Technology Process of 4-MethyluMbelliferyl 2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylMethylene-α-D-galactopyranoside

There total 1 articles about 4-MethyluMbelliferyl 2-Azido-2-deoxy-3-O-(tetra-O-acetyl-β-D-galactopyranosyl)-4,6-O-phenylMethylene-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₁₆H₂₀Cl₃NO₁₀

: 1147438-59-2
4-methylumbelliferyl 2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

: 1147438-61-6
4-methylumbelliferyl 2-azido-4,6-O-benzylidene-2-deoxy-3-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 2h; stereoselective reaction; Molecular sieve;
DOI:10.1016/j.carres.2008.12.013

Reference yield: 40.0%

: 1147438-61-6
4-methylumbelliferyl 2-azido-4,6-O-benzylidene-2-deoxy-3-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranoside

: 108-24-7
acetic anhydride

: 64-19-7,77671-22-8
acetic acid

: 210357-36-1,82358-93-8
4-methylumbelliferyl β-D-galactopyranosyl-(1->3)-2-acetamido-2-deoxy-α-D-galactopyranoside

Guidance literature:: 4-methylumbelliferyl 2-azido-4,6-O-benzylidene-2-deoxy-3-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranoside; With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 ℃; for 2h; under 760.051 Torr;

acetic anhydride; In pyridine; at 20 ℃; for 1h;

acetic acid; Further stages;
DOI:10.1016/j.carres.2008.12.013