pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide]

Base Information

Chemical Name:pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide]
CAS No.:549513-93-1
Molecular Formula:C₂₁H₂₆N₄O₅
Molecular Weight:414.461
Hs Code.:

Synonyms:pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide]

Chemical Property:

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Technology Process of pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide]

There total 2 articles about pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-(N,N-diethylcarbamoyl)pyridine-2-carboxylic acylchloride

: 218143-44-3
N-ethyl-(4-methoxymethyl-2-nitrophenyl)amine

: 549513-93-1
pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide]

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 40 ℃; for 2.16667h;
DOI:10.1002/chem.200390099

Reference yield:

: 179469-06-8
2-(hydroxycarbonyl)-6-[(N,N-diethylamino)carbonyl]pyridine

: 549513-93-1
pyridine-2,6-dicarboxylic acid 2-diethylamide 6-[ethyl-(4-methoxymethyl-2-nitro-phenyl)-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂; DMF / CH₂Cl₂ / 1.5 h / Heating

2: 12.28 g / Et₃N / CH₂Cl₂ / 2.17 h / 0 - 40 °C

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/chem.200390099