(R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate

Base Information

• Chemical Name: (R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate
• CAS No.: 869218-55-3
• Molecular Formula: C₂₃H₃₇BO₂Si
• Molecular Weight: 384.442

Synonyms:(R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate

Chemical Property of (R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate

Chemical Property:

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Technology Process of (R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate

There total 7 articles about (R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(R,R)-1,2-dicyclohexylethane-1,2-diol {(1S)-[(S,S)-N,N-bis(1-phenylethyl)carbamoyloxy](dimethylphenylsilyl)methyl}boronate (869218-53-1) + lithium triethylborohydride (22560-16-3) → (R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate (869218-55-3)

Guidance literature:

In diethyl ether; at 0°C for 30 min;

DOI:10.1021/ja051568g

Reference yield: 81.0%

(R,R)-1,2-dicyclohexylethane-1,2-diol {(R)-[(S,S)-N,N-bis(1-phenylethyl)carbamoyloxy](dimethylphenylsilyl)methyl}boronate (869218-54-2) + lithium triethylborohydride (22560-16-3) → (R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate (869218-55-3)

Guidance literature:

In diethyl ether; at 0°C for 30 min;

DOI:10.1021/ja051568g

Reference yield: 71.0%

(R,R)-1,2-dicyclohexylethane-1,2-diol {(1S)-[(S,S)-N,N-bis(1-phenylethyl)carbamoyloxy](dimethylphenylsilyl)methyl}boronate (869218-53-1) → (R,R)-1,2-dicyclohexylethane-1,2-diol (dimethylphenylsilyl)methylboronate (869218-55-3)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 0.5h;

DOI:10.1021/ja051568g

upstream raw materials:

(R,R)-1,2-dicyclohexylethane-1,2-diol {(1S)-[(S,S)-N,N-bis(1-phenylethyl)carbamoyloxy](dimethylphenylsilyl)methyl}boronate

(R,R)-1,2-dicyclohexylethane-1,2-diol tert-butyl alcohol borate

(dimethylphenylsilyl)methyl (S,S)-N,N-bis(1-phenylethyl)carbamate

(1R,2R)-1,2-dicyclohexyl-1,2-ethanediol

Downstream raw materials:

biphenyl

dimethylphenyl(phenylmethyl)silane

(R,R)-1,2-dicyclohexylethane-1,2-diol {(1R)-[(S,S)-N,N-bis(1-phenylethyl)carbamoyloxy](dimethylphenylsilyl)[1-2H]methyl}boronate

(R,R)-1,2-dicyclohexylethane-1,2-diol {(1S)-[(S,S)-N,N-bis(1-phenylethyl)carbamoyloxy](dimethylphenylsilyl)[1-2H]methyl}boronate

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