5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II)

Base Information

• Chemical Name: 5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II)
• CAS No.: 1314587-52-4
• Molecular Formula: C₆₉H₅₆N₈O₂Zn
• Molecular Weight: 1094.65

Synonyms:5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II)

Chemical Property of 5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II)

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Technology Process of 5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II)

There total 7 articles about 5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-methoxycarboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrin → 5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II) (1314587-52-4)

Guidance literature:

5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-methoxycarboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrin; With zinc(II) acetate dihydrate; In tetrachloromethane; butan-1-ol; for 48h; Inert atmosphere; Reflux;

With sodium hydroxide; In tetrahydrofuran; water; for 16h; Reflux;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1002/cssc.201100029

Reference yield:

12-hydroxyl-5,10,15,20-tetrakis(2,4,6-trimethylphenyl)quinoxalino[2,3-b]porphyrin → 5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II) (1314587-52-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: Dess-Martin periodane / dichloromethane / 4 h / 20 °C / Inert atmosphere

2.1: pyridine / 11 h / 110 °C

3.1: zinc(II) acetate dihydrate / tetrachloromethane; butan-1-ol / 48 h / Inert atmosphere; Reflux

3.2: 16 h / Reflux

3.3: 20 °C

With pyridine; zinc(II) acetate dihydrate; Dess-Martin periodane; In tetrachloromethane; dichloromethane; butan-1-ol;

DOI:10.1002/cssc.201100029

Reference yield:

12-acetoxyl-5,10,15,20-tetrakis(2,4,6-trimethylphenyl)quinoxalino[2,3-b]porphyrin → 5,10,15,20-tetrakis(2,4,6-trimethylphenyl)-6'-carboxylquinoxalino[2,3-b]quinoxalino[12,13-b']porphyrinato zinc(II) (1314587-52-4)

Guidance literature:

Multi-step reaction with 4 steps

1.1: methanol; potassium carbonate / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 4 h / 20 °C / Inert atmosphere

3.1: pyridine / 11 h / 110 °C

4.1: zinc(II) acetate dihydrate / tetrachloromethane; butan-1-ol / 48 h / Inert atmosphere; Reflux

4.2: 16 h / Reflux

4.3: 20 °C

With pyridine; methanol; zinc(II) acetate dihydrate; potassium carbonate; Dess-Martin periodane; In tetrachloromethane; dichloromethane; butan-1-ol;

DOI:10.1002/cssc.201100029

upstream raw materials:

1,2-diamino-benzene

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