(2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole

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Chemical Name:(2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole
CAS No.:134339-87-0
Molecular Formula:C₁₇H₂₉NOSi₂
Molecular Weight:319.594
Hs Code.:

Synonyms:(2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole

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Chemical Property of (2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole

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Technology Process of (2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole

There total 1 articles about (2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 134339-83-6
(Bis-trimethylsilanyl-methyl)-[(E)-3-(2-methoxy-phenyl)-prop-2-en-(E)-ylidene]-amine

: 134339-92-7
(2S,3S)-3-(2-Methoxy-phenyl)-2-trimethylsilanyl-3,4-dihydro-2H-pyrrole

: 134339-87-0
(2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole

Guidance literature:: at 200 ℃; for 0.5h;
DOI:10.1039/c39910000524

Reference yield: 86.0%

: 134339-87-0
(2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole

: 134339-92-7
(2S,3S)-3-(2-Methoxy-phenyl)-2-trimethylsilanyl-3,4-dihydro-2H-pyrrole

Guidance literature:: With chloro-trimethyl-silane; In methanol; at 0 ℃; for 1h;
DOI:10.1039/c39910000524

Reference yield:

: 134339-87-0
(2R,3R)-3-(2-Methoxy-phenyl)-1,2-bis-trimethylsilanyl-2,3-dihydro-1H-pyrrole

: (3,5-Dinitro-phenyl)-[(2R,3R)-3-(2-methoxy-phenyl)-2-trimethylsilanyl-pyrrolidin-1-yl]-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / ClSiMe₃ / methanol / 1 h / 0 °C

2: 82 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

3: NEt₃ / CH₂Cl₂ / 1 h / Ambient temperature

With lithium aluminium tetrahydride; chloro-trimethyl-silane; triethylamine; In methanol; diethyl ether; dichloromethane;
DOI:10.1039/c39910000524