N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide

Base Information

• Chemical Name: N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide
• CAS No.: 1255791-54-8
• Molecular Formula: C₂₉H₄₂N₂O₅S
• Molecular Weight: 530.729

Synonyms:N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide

Chemical Property of N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide

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Technology Process of N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide

There total 1 articles about N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl-(2S,3R)-4-(2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)phenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate (1190426-81-3) → N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide (1255791-54-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

DOI:10.1021/jm900695w

Reference yield:

N-((2R,3S)-3-amino-2-hydroxy-4-phenylbutyl)-2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)benzensulfonamide (1255791-54-8) + (3R,3aS,6aR)-hexahydrofuro[2,3-b]furan-3-yl-(4-nitrophenyl)carbonic acid (192725-55-6,252873-01-1,252873-35-1) → (3R,3aS,6aR)-hexahydrofuro[2,3-b]furan-3-yl (2S,3R)-4-(2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)phenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate (1190426-84-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm900695w

upstream raw materials:

tert-butyl-(2S,3R)-4-(2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)phenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate

Downstream raw materials:

(3R,3aS,6aR)-hexahydrofuro[2,3-b]furan-3-yl (2S,3R)-4-(2-(hex-5-enyloxy)-4-methoxy-N-((S)-2-methylpent-4-enyl)phenylsulfonamido)-3-hydroxy-1-phenylbutan-2-ylcarbamate

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